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1 article(s) from Breindahl, Torben

Synthesis and stability study of a new major metabolite of γ-hydroxybutyric acid

Ida Nymann Petersen,
Jesper Langgaard Kristensen,
Christian Tortzen,
Torben Breindahl and
Daniel Sejer Pedersen

Beilstein J. Org. Chem. 2013, 9, 641–646, doi:10.3762/bjoc.9.72

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Figure 1: Hypothesised glucuronidation of GHB (1) by UDP-glucuronosyltransferase to give glucuronide 2. UDP =...

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Scheme 1: Schmidt glucuronidation [11] with trichloroacetimidate 3. Synthesis of 4 and 5 using acceptors 7 and 8 ...

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Scheme 2: Koenigs–Knorr glucuronidation [27] with bromide 10 and acceptors 7 and 8.

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Scheme 3: Synthesis of GHB glucuronides 2 and d₄-2 by using a Koenigs–Knorr glucuronidation approach. TEMPO: ...

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Figure 2: ¹H NMR spectrum (D₂O, 300 MHz) of GHB glucuronides 2 (top) and d₄-2 (bottom). As anticipated, methy...

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Figure 3: ¹H NMR spectra (500 MHz) of GHB glucuronide 2 in pH 4.8 buffer at t = 0 (rt) and t = 72 h (90 °C) b...

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Published 02 Apr 2013

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